TA Instruments

AR1699-0001f

04/09/2012 15:27:44

Sample name	ASW 10 mm from base, 60 mm to top, disk 14 PMMA+FA clean
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1699
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 15:27:44

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-31.73	6.020	-5.271	1.0080	22.4	112.4	2.4914	10000	0.02759	3.102	3.1143	311.43	3.384E-3	0.0	1.0	61.008	-97.360	4.816
0.7677	12.82	0.05988	2.0080	22.4	116.6	13.9918	10000	0.02861	0.7091	17.490	1749.0	3.384E-3	0.0	1.0	62.008	2.3553	10.26
1.543	19.60	0.07872	3.0120	22.4	107.5	27.5891	10000	0.02638	0.2796	34.486	3448.6	3.384E-3	0.1	1.1	63.012	4.7347	15.68
2.092	23.23	0.09006	4.0120	22.4	107.5	41.4726	10000	0.02638	0.1992	51.841	5184.1	3.383E-3	0.1	1.1	64.012	6.4184	18.58
3.443	30.97	0.1112	5.0080	22.4	100.0	68.0529	10000	0.02455	0.1043	85.066	8506.6	3.384E-3	0.1	1.1	65.008	10.563	24.78
5.301	39.58	0.1339	6.0120	22.4	119.0	107.1650	10000	0.02922	0.07597	133.96	13396	3.384E-3	0.1	1.1	66.012	16.262	31.67
5.947	42.63	0.1395	7.0080	22.4	106.6	127.0910	10000	0.02617	0.05868	158.86	15886	3.384E-3	0.1	1.1	67.008	18.244	34.10
7.489	49.21	0.1522	8.0080	22.4	119.0	165.7480	10000	0.02922	0.04916	207.19	20719	3.383E-3	0.1	1.1	68.008	22.977	39.36
10.04	57.60	0.1742	9.0080	22.4	106.6	223.6330	10000	0.02617	0.03214	279.54	27954	3.383E-3	0.2	1.2	69.008	30.792	46.08
11.96	63.75	0.1876	9.9920	22.4	98.37	275.4050	10000	0.02414	0.02420	344.26	34426	3.384E-3	0.2	1.2	69.992	36.701	51.00
13.89	69.70	0.1993	11.004	22.4	92.59	326.4950	10000	0.02272	0.01906	408.12	40812	3.383E-3	0.2	1.2	71.004	42.614	55.76
15.68	75.17	0.2086	11.996	22.4	92.59	378.2030	10000	0.02272	0.01639	472.75	47275	3.383E-3	0.2	1.2	71.996	48.118	60.14
17.38	80.56	0.2157	12.992	22.4	101.7	435.4320	10000	0.02496	0.01567	544.29	54429	3.383E-3	0.2	1.2	72.992	53.312	64.45
19.53	86.47	0.2259	13.988	22.4	95.89	499.0600	10000	0.02354	0.01282	623.83	62383	3.383E-3	0.2	1.2	73.988	59.922	69.18
22.65	94.64	0.2393	15.008	22.4	76.05	594.6230	10000	0.01867	8.491E-3	743.28	74328	3.384E-3	0.3	1.3	75.008	69.493	75.71
25.08	99.95	0.2509	16.008	22.4	85.97	664.6900	10000	0.02110	8.606E-3	830.86	83086	3.384E-3	0.3	1.3	76.008	76.931	79.96
26.98	105.7	0.2552	17.008	22.4	79.36	741.1490	10000	0.01948	7.103E-3	926.44	92644	3.384E-3	0.3	1.3	77.008	82.772	84.56
30.53	113.8	0.2684	18.008	22.4	79.36	856.2580	10000	0.01948	6.132E-3	1070.3	1.0703E5	3.383E-3	0.3	1.3	78.008	93.662	91.01
32.90	118.8	0.2769	19.008	22.4	79.36	931.6540	10000	0.01948	5.620E-3	1164.6	1.1646E5	3.383E-3	0.3	1.3	79.008	100.94	95.06
35.35	124.3	0.2844	19.992	22.4	62.00	1020.9400	10000	0.01522	4.014E-3	1276.2	1.2762E5	3.384E-3	0.3	1.3	79.992	108.46	99.43
38.89	132.3	0.2939	21.008	22.4	77.71	1154.3199	10000	0.01907	4.438E-3	1442.9	1.4429E5	3.384E-3	0.4	1.4	81.008	119.30	105.9
41.47	137.4	0.3018	21.996	22.4	66.96	1242.6200	10000	0.01643	3.547E-3	1553.3	1.5533E5	3.384E-3	0.4	1.4	81.996	127.23	109.9
44.07	142.8	0.3086	23.008	22.4	56.21	1344.0300	10000	0.01380	2.756E-3	1680.0	1.6800E5	3.384E-3	0.4	1.4	83.008	135.22	114.3
47.62	150.8	0.3157	24.008	22.4	65.31	1496.1300	10000	0.01603	2.870E-3	1870.2	1.8702E5	3.383E-3	0.4	1.4	84.008	146.09	120.7
50.19	155.9	0.3218	25.004	22.4	68.61	1598.5000	10000	0.01684	2.822E-3	1998.1	1.9981E5	3.384E-3	0.4	1.4	85.004	153.97	124.8
53.32	161.3	0.3304	26.008	22.4	65.31	1711.4500	10000	0.01603	2.509E-3	2139.3	2.1393E5	3.384E-3	0.4	1.4	86.008	163.57	129.1
57.89	169.3	0.3419	27.008	22.4	46.29	1883.5400	10000	0.01136	1.614E-3	2354.4	2.3544E5	3.384E-3	0.5	1.5	87.008	177.61	135.5
60.50	174.5	0.3468	28.008	22.4	50.43	1996.8500	10000	0.01238	1.657E-3	2496.1	2.4961E5	3.384E-3	0.5	1.5	88.008	185.60	139.6
63.23	179.6	0.3521	28.992	22.4	42.99	2118.4500	10000	0.01055	1.333E-3	2648.1	2.6481E5	3.384E-3	0.5	1.5	88.992	193.97	143.7
68.09	187.6	0.3630	29.992	22.4	48.77	2306.0901	10000	0.01197	1.386E-3	2882.6	2.8826E5	3.383E-3	0.5	1.5	89.992	208.91	150.1
71.45	192.7	0.3708	30.992	22.4	34.72	2432.7400	10000	8.521E-3	9.348E-4	3040.9	3.0409E5	3.384E-3	0.5	1.5	90.992	219.22	154.2
74.07	197.8	0.3744	31.992	22.4	28.11	2565.4800	10000	6.898E-3	7.180E-4	3206.9	3.2069E5	3.384E-3	0.5	1.5	91.992	227.26	158.3
79.93	205.8	0.3883	33.008	22.4	28.11	2774.1001	10000	6.898E-3	6.634E-4	3467.6	3.4676E5	3.384E-3	0.6	1.6	93.008	245.21	164.7
82.73	211.0	0.3921	34.008	22.4	19.84	2913.0100	10000	4.869E-3	4.456E-4	3641.3	3.6413E5	3.384E-3	0.6	1.6	94.008	253.83	168.8
88.49	218.6	0.4048	35.008	22.4	10.75	3127.9299	10000	2.638E-3	2.249E-4	3909.9	3.9099E5	3.384E-3	0.6	1.6	95.008	271.47	174.9
90.53	223.9	0.4043	36.008	22.4	5.787	3279.5100	10000	1.420E-3	1.154E-4	4099.4	4.0994E5	3.384E-3	0.6	1.6	96.008	277.75	179.1
93.70	229.1	0.4090	37.008	22.4	-10.75	3507.6899	10000	-2.638E-3	-2.048E-4	4384.6	4.3846E5	3.383E-3	0.6	1.6	97.008	287.46	183.3
99.48	236.6	0.4204	37.992	22.4	8.267	3658.8201	10000	2.029E-3	1.476E-4	4573.5	4.5735E5	3.384E-3	0.6	1.6	97.992	305.19	189.3
102.9	241.8	0.4256	39.008	22.4	-1.45E-11	3822.6599	10000	-3.55E-15	-2.47E-16	4778.3	4.7783E5	3.384E-3	0.7	1.7	99.008	315.77	193.5
108.6	249.6	0.4353	40.008	22.4	9.093	4068.9500	10000	2.232E-3	1.460E-4	5086.2	5.0862E5	3.384E-3	0.7	1.7	100.008	333.33	199.7
112.7	254.6	0.4428	41.008	22.4	-5.787	4234.0298	10000	-1.420E-3	-8.925E-5	5292.5	5.2925E5	3.384E-3	0.7	1.7	101.008	345.89	203.7
115.4	259.9	0.4440	41.996	22.4	-15.71	4410.0298	10000	-3.855E-3	-2.326E-4	5512.5	5.5125E5	3.383E-3	0.7	1.7	101.996	353.99	207.9
120.8	267.6	0.4514	43.008	22.4	-20.67	4674.9600	10000	-5.072E-3	-2.885E-4	5843.7	5.8437E5	3.383E-3	0.7	1.7	103.008	370.64	214.1
124.7	272.7	0.4574	44.004	22.4	-40.51	4851.7202	10000	-9.942E-3	-5.448E-4	6064.7	6.0647E5	3.383E-3	0.7	1.7	104.004	382.65	218.1
128.8	280.4	0.4594	45.008	22.4	-21.49	5129.3398	10000	-5.275E-3	-2.734E-4	6411.7	6.4117E5	3.384E-3	0.8	1.8	105.008	395.16	224.3
133.7	285.5	0.4682	46.012	22.4	-29.76	5320.0000	10000	-7.304E-3	-3.650E-4	6650.0	6.6500E5	3.383E-3	0.8	1.8	106.012	410.12	228.4
141.2	293.1	0.4818	47.008	22.4	-38.85	5604.4302	10000	-9.536E-3	-4.522E-4	7005.5	7.0055E5	3.383E-3	0.8	1.8	107.008	433.29	234.5
144.7	298.3	0.4851	48.008	22.4	-62.00	5804.4302	10000	-0.01522	-6.967E-4	7255.5	7.2555E5	3.384E-3	0.8	1.8	108.008	443.95	238.7
147.9	303.5	0.4873	49.004	22.4	-64.48	6006.2700	10000	-0.01583	-7.000E-4	7507.8	7.5078E5	3.384E-3	0.8	1.8	109.004	453.74	242.8
154.4	311.1	0.4961	49.992	22.4	-50.43	6308.9800	10000	-0.01238	-5.209E-4	7886.2	7.8862E5	3.384E-3	0.8	1.8	109.992	473.59	248.9
157.9	316.2	0.4994	50.996	22.4	-55.39	6517.2700	10000	-0.01359	-5.540E-4	8146.6	8.1466E5	3.383E-3	0.8	1.8	110.996	484.42	252.9
163.9	324.0	0.5058	51.996	22.4	-68.61	6842.5801	10000	-0.01684	-6.538E-4	8553.2	8.5532E5	3.383E-3	0.9	1.9	111.996	502.69	259.2
167.7	329.0	0.5097	52.992	22.4	-81.01	7053.2900	10000	-0.01988	-7.483E-4	8816.6	8.8166E5	3.384E-3	0.9	1.9	112.992	514.54	263.2
173.8	336.6	0.5164	54.004	22.4	-50.43	7384.4199	10000	-0.01238	-4.451E-4	9230.5	9.2305E5	3.384E-3	0.9	1.9	114.004	533.20	269.3
180.0	341.7	0.5267	55.008	22.4	-45.47	7608.1201	10000	-0.01116	-3.893E-4	9510.2	9.5102E5	3.384E-3	0.9	1.9	115.008	552.20	273.4
182.6	346.9	0.5265	55.992	22.4	-64.48	7835.2100	10000	-0.01583	-5.360E-4	9794.0	9.7940E5	3.383E-3	0.9	1.9	115.992	560.25	277.5
189.9	354.4	0.5360	57.008	22.4	-100.9	8175.7002	10000	-0.02475	-8.031E-4	10220	1.0220E6	3.384E-3	1.0	2.0	117.008	582.72	283.5
193.9	359.5	0.5393	58.012	22.4	-100.0	8415.1699	10000	-0.02455	-7.740E-4	10519	1.0519E6	3.383E-3	1.0	2.0	118.012	594.80	287.6
199.7	367.1	0.5439	59.004	22.4	-90.93	8774.6104	10000	-0.02232	-6.747E-4	10968	1.0968E6	3.384E-3	1.0	2.0	119.004	612.59	293.7
205.6	372.1	0.5526	59.992	22.4	-74.40	9014.1396	10000	-0.01826	-5.372E-4	11268	1.1268E6	3.384E-3	1.0	2.0	119.992	630.89	297.7

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

211.2	375.0	0.5633	1.0040	22.4	-92.59	209.8220	10000	-0.02272	-6.584E-4	262.28	26228	3.384E-3	0.0	2.0	121.004	648.10	300.0
209.1	375.0	0.5575	2.0000	22.4	-75.23	587.0390	10000	-0.01846	-5.350E-4	733.80	73380	3.384E-3	0.0	2.0	122.000	641.41	300.0
210.0	375.0	0.5600	3.0040	22.4	-100.0	838.2110	10000	-0.02455	-7.113E-4	1047.8	1.0478E5	3.383E-3	0.1	2.1	123.004	644.29	300.0
209.5	375.0	0.5586	4.0080	22.4	-103.3	1089.6000	10000	-0.02536	-7.348E-4	1362.0	1.3620E5	3.384E-3	0.1	2.1	124.008	642.63	300.0
211.4	375.0	0.5637	5.0040	22.4	-79.36	1466.5100	10000	-0.01948	-5.643E-4	1833.1	1.8331E5	3.384E-3	0.1	2.1	125.004	648.47	300.0
208.2	375.0	0.5552	6.0200	22.4	-96.72	1717.9200	10000	-0.02374	-6.878E-4	2147.4	2.1474E5	3.383E-3	0.1	2.1	126.020	638.76	300.0
209.9	375.0	0.5597	7.0040	22.4	-106.6	2094.8000	10000	-0.02617	-7.583E-4	2618.5	2.6185E5	3.383E-3	0.1	2.1	127.004	643.88	300.0
210.7	375.0	0.5619	8.0080	22.4	-50.43	2346.2400	10000	-0.01238	-3.586E-4	2932.8	2.9328E5	3.384E-3	0.1	2.1	128.008	646.45	300.0
209.7	375.0	0.5593	9.0040	22.4	-87.62	2727.1299	10000	-0.02151	-6.231E-4	3408.9	3.4089E5	3.384E-3	0.2	2.2	129.004	643.45	300.0
213.2	375.0	0.5685	10.020	22.4	-119.9	2974.4600	10000	-0.02942	-8.524E-4	3718.1	3.7181E5	3.384E-3	0.2	2.2	130.020	654.08	300.0
207.4	375.0	0.5531	11.004	22.4	-62.00	3227.4399	10000	-0.01522	-4.409E-4	4034.3	4.0343E5	3.383E-3	0.2	2.2	131.004	636.33	300.0
214.2	375.0	0.5712	12.008	22.4	-121.5	3618.1001	10000	-0.02983	-8.642E-4	4522.6	4.5226E5	3.383E-3	0.2	2.2	132.008	657.10	300.0
212.3	375.0	0.5661	13.004	22.4	-119.0	3854.0300	10000	-0.02922	-8.465E-4	4817.5	4.8175E5	3.383E-3	0.2	2.2	133.004	651.29	300.0
210.3	375.0	0.5609	14.004	22.4	-85.15	4105.5898	10000	-0.02090	-6.055E-4	5132.0	5.1320E5	3.384E-3	0.2	2.2	134.004	645.35	300.0
208.2	375.0	0.5551	15.004	22.4	-67.79	4482.5898	10000	-0.01664	-4.820E-4	5603.2	5.6032E5	3.384E-3	0.3	2.3	135.004	638.65	300.0
210.1	375.0	0.5604	16.004	22.4	-100.0	4735.6899	10000	-0.02455	-7.113E-4	5919.6	5.9196E5	3.383E-3	0.3	2.3	136.004	644.72	300.0
210.6	375.0	0.5617	17.012	22.4	-85.97	5111.9600	10000	-0.02110	-6.114E-4	6390.0	6.3900E5	3.383E-3	0.3	2.3	137.012	646.22	300.0
210.4	375.0	0.5610	18.004	22.4	-124.0	5364.3999	10000	-0.03043	-8.818E-4	6705.5	6.7055E5	3.384E-3	0.3	2.3	138.004	645.47	300.0
210.9	375.0	0.5623	19.000	22.4	-109.1	5613.3901	10000	-0.02678	-7.759E-4	7016.7	7.0167E5	3.384E-3	0.3	2.3	139.000	646.90	300.0
208.0	375.0	0.5548	20.004	22.4	-107.5	5990.3599	10000	-0.02638	-7.642E-4	7488.0	7.4880E5	3.384E-3	0.3	2.3	140.004	638.25	300.0
210.2	375.0	0.5605	21.004	22.4	-88.45	6241.7998	10000	-0.02171	-6.290E-4	7802.3	7.8023E5	3.384E-3	0.4	2.4	141.004	644.79	300.0
209.9	375.0	0.5597	22.004	22.4	-96.72	6620.4502	10000	-0.02374	-6.878E-4	8275.6	8.2756E5	3.383E-3	0.4	2.4	142.004	643.86	300.0
207.8	375.0	0.5541	23.004	22.4	-109.9	6870.2202	10000	-0.02698	-7.818E-4	8587.8	8.5878E5	3.383E-3	0.4	2.4	143.004	637.47	300.0
209.5	375.0	0.5587	24.020	22.4	-90.93	7121.5098	10000	-0.02232	-6.467E-4	8901.9	8.9019E5	3.383E-3	0.4	2.4	144.020	642.80	300.0
208.3	375.0	0.5555	25.004	22.4	-114.9	7498.5200	10000	-0.02820	-8.171E-4	9373.2	9.3732E5	3.383E-3	0.4	2.4	145.004	639.07	300.0
209.1	375.0	0.5575	26.000	22.4	-101.7	7749.8501	10000	-0.02496	-7.231E-4	9687.3	9.6873E5	3.384E-3	0.4	2.4	146.000	641.43	300.0
209.4	375.0	0.5584	27.020	22.4	-96.72	8000.9502	10000	-0.02374	-6.878E-4	10001	1.0001E6	3.383E-3	0.5	2.5	147.020	642.48	300.0
209.5	375.0	0.5587	28.004	22.4	-107.5	8378.0498	10000	-0.02638	-7.642E-4	10473	1.0473E6	3.383E-3	0.5	2.5	148.004	642.77	300.0
209.6	375.0	0.5589	29.004	22.4	-104.2	8629.4199	10000	-0.02556	-7.406E-4	10787	1.0787E6	3.384E-3	0.5	2.5	149.004	643.02	300.0
205.5	375.0	0.5479	30.016	22.4	-76.88	9006.3398	10000	-0.01887	-5.467E-4	11258	1.1258E6	3.384E-3	0.5	2.5	150.016	630.41	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

206.0	371.7	0.5542	1.0040	22.4	-77.71	245.4810	10000	-0.01907	-5.626E-4	306.85	30685	3.383E-3	0.0	2.5	152.004	631.95	297.3
198.7	364.2	0.5458	2.0240	22.4	-85.97	602.0690	10000	-0.02110	-6.483E-4	752.59	75259	3.384E-3	0.0	2.6	153.024	609.73	291.3
192.9	359.1	0.5373	3.0240	22.4	-62.83	839.8250	10000	-0.01542	-4.873E-4	1049.8	1.0498E5	3.384E-3	0.1	2.6	154.024	591.88	287.2
189.8	353.9	0.5362	4.0040	22.4	-40.51	1079.7400	10000	-9.942E-3	-3.234E-4	1349.7	1.3497E5	3.384E-3	0.1	2.6	155.004	582.19	283.1
181.7	346.4	0.5245	5.0200	22.4	-53.73	1421.3400	10000	-0.01319	-4.479E-4	1776.7	1.7767E5	3.384E-3	0.1	2.6	156.020	557.30	277.1
180.8	341.3	0.5299	6.0240	22.4	-83.49	1641.6400	10000	-0.02049	-7.168E-4	2052.1	2.0521E5	3.384E-3	0.1	2.6	157.024	554.78	273.0
173.0	333.5	0.5188	7.0040	22.4	-67.79	1982.1700	10000	-0.01664	-6.093E-4	2477.7	2.4777E5	3.384E-3	0.1	2.6	158.004	530.84	266.8
167.5	328.5	0.5100	8.0040	22.4	-52.91	2192.5801	10000	-0.01299	-4.903E-4	2740.7	2.7407E5	3.383E-3	0.1	2.7	159.004	513.98	262.8
161.7	320.9	0.5041	9.0200	22.4	-55.39	2511.7700	10000	-0.01359	-5.379E-4	3139.7	3.1397E5	3.384E-3	0.2	2.7	160.020	496.22	256.7
158.3	315.7	0.5013	10.020	22.4	-62.83	2730.4900	10000	-0.01542	-6.303E-4	3413.1	3.4131E5	3.384E-3	0.2	2.7	161.020	485.54	252.6
155.2	310.5	0.4998	11.004	22.4	-58.69	2931.2200	10000	-0.01441	-6.087E-4	3664.0	3.6640E5	3.384E-3	0.2	2.7	162.004	476.17	248.4
149.9	302.9	0.4949	12.020	22.4	-35.55	3231.8401	10000	-8.724E-3	-3.873E-4	4039.8	4.0398E5	3.383E-3	0.2	2.7	163.020	459.99	242.4
142.9	297.8	0.4799	13.036	22.4	-28.11	3431.8301	10000	-6.898E-3	-3.170E-4	4289.8	4.2898E5	3.384E-3	0.2	2.7	164.036	438.40	238.2
139.0	290.1	0.4791	14.004	22.4	-14.05	3721.0000	10000	-3.449E-3	-1.670E-4	4651.3	4.6513E5	3.384E-3	0.2	2.8	165.004	426.43	232.1
134.4	285.1	0.4715	15.020	22.4	-11.57	3907.3201	10000	-2.840E-3	-1.424E-4	4884.2	4.8842E5	3.383E-3	0.3	2.8	166.020	412.43	228.1
127.6	277.3	0.4603	16.004	22.4	-9.093	4189.8301	10000	-2.232E-3	-1.182E-4	5237.3	5.2373E5	3.384E-3	0.3	2.8	167.004	391.62	221.9
123.7	272.1	0.4546	17.008	22.4	-2.480	4370.3301	10000	-6.087E-4	-3.348E-5	5462.9	5.4629E5	3.384E-3	0.3	2.8	168.008	379.53	217.7
121.3	267.1	0.4541	18.016	22.4	-18.19	4545.3901	10000	-4.464E-3	-2.549E-4	5681.7	5.6817E5	3.383E-3	0.3	2.8	169.016	372.14	213.7
115.8	259.4	0.4462	19.004	22.4	-4.960	4808.9600	10000	-1.217E-3	-7.371E-5	6011.2	6.0112E5	3.383E-3	0.3	2.8	170.004	355.13	207.5
111.1	254.1	0.4371	20.012	22.4	19.01	4983.1602	10000	4.666E-3	2.944E-4	6229.0	6.2290E5	3.383E-3	0.3	2.9	171.012	340.78	203.3
106.2	246.5	0.4310	21.024	22.4	20.67	5227.4600	10000	5.072E-3	3.401E-4	6534.3	6.5343E5	3.383E-3	0.4	2.9	172.024	325.96	197.2
101.9	241.3	0.4222	22.004	22.4	22.32	5389.5801	10000	5.478E-3	3.832E-4	6737.0	6.7370E5	3.384E-3	0.4	2.9	173.004	312.60	193.1
98.90	236.1	0.4190	23.004	22.4	27.28	5552.7700	10000	6.695E-3	4.895E-4	6941.0	6.9410E5	3.383E-3	0.4	2.9	174.004	303.42	188.9
93.36	228.5	0.4086	24.004	22.4	21.49	5777.1001	10000	5.275E-3	4.117E-4	7221.4	7.2214E5	3.384E-3	0.4	2.9	175.004	286.42	182.8
91.79	223.3	0.4110	25.012	22.4	22.32	5927.1099	10000	5.478E-3	4.475E-4	7408.9	7.4089E5	3.383E-3	0.4	2.9	176.012	281.61	178.7
86.94	218.1	0.3986	26.004	22.4	22.32	6154.0801	10000	5.478E-3	4.693E-4	7692.6	7.6926E5	3.383E-3	0.4	3.0	177.004	266.72	174.5
81.98	210.3	0.3898	27.004	22.4	41.33	6289.4800	10000	0.01014	9.346E-4	7861.9	7.8619E5	3.383E-3	0.5	3.0	178.004	251.50	168.2
79.08	205.2	0.3854	28.020	22.4	36.37	6429.0601	10000	8.927E-3	8.640E-4	8036.3	8.0363E5	3.383E-3	0.5	3.0	179.020	242.61	164.1
73.70	197.3	0.3736	29.008	22.4	52.91	6633.9600	10000	0.01299	1.360E-3	8292.5	8.2925E5	3.383E-3	0.5	3.0	180.008	226.11	157.8
69.72	192.2	0.3628	30.004	22.4	50.43	6757.8398	10000	0.01238	1.366E-3	8447.3	8.4473E5	3.383E-3	0.5	3.0	181.004	213.91	153.7
66.66	184.5	0.3613	31.004	22.4	40.51	6945.7798	10000	9.942E-3	1.190E-3	8682.2	8.6822E5	3.384E-3	0.5	3.0	182.004	204.51	147.6
63.11	179.2	0.3522	32.004	22.4	39.68	7069.9302	10000	9.739E-3	1.236E-3	8837.4	8.8374E5	3.384E-3	0.5	3.1	183.004	193.61	143.3
60.13	173.8	0.3459	33.004	22.4	46.29	7189.7100	10000	0.01136	1.532E-3	8987.1	8.9871E5	3.384E-3	0.6	3.1	184.004	184.47	139.1
55.57	166.2	0.3344	34.004	22.4	58.69	7356.8999	10000	0.01441	2.126E-3	9196.1	9.1961E5	3.384E-3	0.6	3.1	185.004	170.49	132.9
52.09	160.9	0.3238	35.004	22.4	73.57	7469.1802	10000	0.01806	2.843E-3	9336.5	9.3365E5	3.383E-3	0.6	3.1	186.004	159.81	128.7
49.44	155.5	0.3179	36.016	22.4	66.13	7575.0698	10000	0.01623	2.734E-3	9468.8	9.4688E5	3.384E-3	0.6	3.1	187.016	151.68	124.4
46.34	147.9	0.3133	37.020	22.4	76.05	7724.6602	10000	0.01867	3.477E-3	9655.8	9.6558E5	3.384E-3	0.6	3.1	188.020	142.17	118.3
43.92	142.6	0.3080	38.020	22.4	49.60	7824.3501	10000	0.01217	2.440E-3	9780.4	9.7804E5	3.384E-3	0.6	3.2	189.020	134.74	114.1
40.97	137.1	0.2989	39.004	22.4	82.67	7923.8701	10000	0.02029	4.400E-3	9904.8	9.9048E5	3.384E-3	0.7	3.2	190.004	125.71	109.7
36.90	129.3	0.2854	40.000	22.4	77.71	8054.6602	10000	0.01907	4.648E-3	10068	1.0068E6	3.383E-3	0.7	3.2	191.000	113.20	103.4
35.08	124.0	0.2830	41.016	22.4	88.45	8141.7300	10000	0.02171	5.755E-3	10177	1.0177E6	3.383E-3	0.7	3.2	192.016	107.62	99.18
32.80	118.4	0.2770	42.020	22.4	76.88	8228.7695	10000	0.01887	5.483E-3	10286	1.0286E6	3.384E-3	0.7	3.2	193.020	100.62	94.73
28.83	110.7	0.2605	43.016	22.4	100.9	8340.5498	10000	0.02475	8.237E-3	10426	1.0426E6	3.384E-3	0.7	3.2	194.016	88.442	88.52
26.53	105.3	0.2519	44.020	22.4	100.0	8415.0596	10000	0.02455	9.019E-3	10519	1.0519E6	3.384E-3	0.7	3.3	195.020	81.396	84.25
24.41	99.69	0.2448	45.000	22.4	95.07	8489.5000	10000	0.02333	9.565E-3	10612	1.0612E6	3.383E-3	0.8	3.3	196.000	74.875	79.75
21.28	91.93	0.2315	46.020	22.4	94.24	8582.5498	10000	0.02313	0.01115	10728	1.0728E6	3.384E-3	0.8	3.3	197.020	65.299	73.54
19.08	86.55	0.2204	47.016	22.4	91.76	8644.4502	10000	0.02252	0.01225	10806	1.0806E6	3.384E-3	0.8	3.3	198.016	58.538	69.24
17.29	80.84	0.2139	48.004	22.4	102.5	8706.5195	10000	0.02516	0.01569	10883	1.0883E6	3.384E-3	0.8	3.3	199.004	53.049	64.67
14.80	75.02	0.1972	49.012	22.4	97.54	8761.8496	10000	0.02394	0.01733	10952	1.0952E6	3.384E-3	0.8	3.3	200.012	45.392	60.01
13.70	69.73	0.1965	50.004	22.4	100.9	8836.7002	10000	0.02475	0.02074	11046	1.1046E6	3.383E-3	0.8	3.4	201.004	42.033	55.79
10.55	60.98	0.1729	51.016	22.4	113.3	8885.1504	10000	0.02780	0.03045	11106	1.1106E6	3.383E-3	0.9	3.4	202.016	32.356	48.79
9.099	54.85	0.1659	52.004	22.4	101.7	8927.8701	10000	0.02496	0.03380	11160	1.1160E6	3.384E-3	0.9	3.4	203.004	27.916	43.88
7.545	49.38	0.1528	53.016	22.4	95.89	8964.6104	10000	0.02354	0.03933	11206	1.1206E6	3.384E-3	0.9	3.4	204.016	23.147	39.50
6.103	43.27	0.1411	54.016	22.4	103.3	9001.0801	10000	0.02536	0.05519	11251	1.1251E6	3.384E-3	0.9	3.4	205.016	18.725	34.61
4.719	36.85	0.1281	55.016	22.4	103.3	9031.2998	10000	0.02536	0.07608	11289	1.1289E6	3.384E-3	0.9	3.4	206.016	14.478	29.48
3.583	31.35	0.1143	56.004	22.4	109.1	9055.4102	10000	0.02678	0.1110	11319	1.1319E6	3.384E-3	0.9	3.5	207.004	10.993	25.08
2.430	24.77	0.09810	56.996	22.4	94.24	9079.0098	10000	0.02313	0.1536	11349	1.1349E6	3.384E-3	0.9	3.5	207.996	7.4559	19.82
1.827	17.38	0.1051	58.004	22.4	98.37	9096.3799	10000	0.02414	0.3255	11370	1.1370E6	3.384E-3	1.0	3.5	209.004	5.6056	13.91
1.067	14.55	0.07330	59.016	22.4	101.7	9102.0195	10000	0.02496	0.4802	11378	1.1378E6	3.384E-3	1.0	3.5	210.016	3.2723	11.64
0.4199	7.939	0.05288	60.004	22.4	114.9	9110.1299	10000	0.02820	1.823	11388	1.1388E6	3.384E-3	1.0	3.5	211.004	1.2881	6.351

